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Beilstein J. Org. Chem. 2013, 9, 1791–1796, doi:10.3762/bjoc.9.208
Graphical Abstract
Scheme 1: Giese reaction using borohydride-based radical mediators.
Figure 1: Pictures of the flow microreactor system (MiChS® System X-1), a micromixer (MiChS β-150, channel wi...
Scheme 2: First screening for the reaction of 1a at different temperatures (90–110 °C) and residence times (2...
Scheme 3: Background reduction of 1a with NaBH3CN.
Scheme 4: Second screening at 70 °C and residence time (5–20 min) in the presence of V-65.
Figure 2: Structures of V-65 and AIBN and their ten hour half-life decomposition temperature.
Scheme 5: Cyanoborohydride mediated Giese reaction of 1b and 1c with ethyl acrylate.